40 CFR § 761.253
Chemical analysis
June 9, 2020
(a) Extract PCBs from the standard wipe sample collection medium and clean-up the extracted PCBs in accordance with either Method 3500B/3540C or Method 3500B/3550B from EPA's SW-846, Test Methods for Evaluating Solid Waste, or a method validated under subpart Q of this part. Use Method 8082 from SW-846, or a method validated under subpart Q of this part, to analyze these extracts for PCBs.
(b) Report all PCB sample concentrations in µg/100 cm2 (16 square inches) of surface sampled. If sampling an area smaller than 100 cm2, report converted sample concentrations in accordance with §761.243(b).